Tuesday, April 22, 2014

Interpreting Solubility Curves






Combustion of a Candle Lab

Purpose: 
To observe a burning candle and calculate the heat associated with the combustion reaction. 

Procedure: 
1) Measure and record the length of a candle in centimeters. 
2) Place the candle on a small piece of aluminum foil and measure the mass of the foil-candle system. 
3) Note the time as you light the candle. Let the candle burn for about five minutes. 
4) Extinguish the candle and record the time. 
5) Measure the mass of the foil-candle system again.

Data: 


Analyze and Conclude: 
1) 
2) The wick is the one that is burning. 
3) The wax is there to hold the wick in place. 
4) The air on top of the candle is hotter because heat rises. 
5) The candle lost 1.2 centimeters and lost .3 grams. For length it would be mostly the wax and for mass it would be the wick. 
6) The wick acts as towel and soaks up the wax. Then the wax and wick burn. 
7) C20 H42 30 1/2 O2 ---> 20CO2 + 21H2O 
8) 1.16g (1mol/282g) = .00411348 mol 

Thursday, April 3, 2014

Heat of Fusion of Ice

Purpose: Determine the heat of fusion of ice

Procedure:
1) Start with 100ml H2O at 50° C
2) Place into calorimeter (styrofoam cup) -record temp
3) Draw two or three ice cubes in and stir, don't run out of ice
4) Once temp stabilizes around 0°C remove ice (unmelted)
5) Measure new volume

Data: 


Calculations:
1) Mass of 100kk H2O =100g
2) Cal q= m*^t*c   =   Q= 100g * 50° C * 4.18 kj/mol
3) Determine q ice  =  16.720 kj/mol
4) Mass of ice melted = 80g H2O
5) Mole of melted ice = 4.4 mol H2O
6) ^ H of fusion for ice = 16,720/ 1000= 16.72 kj/mol
16.72/4.4 mol = 3.8 kj/mol
 
Conclusion:
Our heat of fusion was 3.8kj/mol. The final result had 36.7% error. We let the ice sit in the water for a while before we took the temperature which made a difference on the result.